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Beilstein J. Org. Chem. 2019, 15, 2398–2407, doi:10.3762/bjoc.15.232
Graphical Abstract
Scheme 1: Reversible photoisomerization of phenylazotrimethylpyrazole 1.
Figure 1: 1H NMR spectrum of (E-1)22 (500 MHz, D2O, 298 K).
Figure 2: Partial 1H-1H NOESY NMR spectrum of (E-1)22 showing NOE correlations between host 2 and guest 1 (50...
Figure 3: Front view (a) and side view (b) of the X-ray crystal structure of (E-1)22 (major conformations of 1...
Figure 4: UV–vis absorption spectrum of an aqueous solution of (E-1)22 (blue) and following exposure of this ...
Figure 5: Top view (a) and side view (b) of the energy-optimized structure of (Z-1)2. Color codes: C, gray; N...
Figure 6: A series of 1H NMR spectra of (E-1)22 (500 MHz, D2O, 298 K) before (bottom) and after exposure to U...
Figure 7: 1H NMR and 1H DOSY spectra of (E-1)22 (500 MHz, D2O, 298 K) before (left) and after (center) UV irr...
Figure 8: Palladium-accelerated back-isomerization of Z-1. a) Kinetics of the thermal back-isomerization of Z-...